Sugar hydrazones 4-7 were prepared through condensation of the respective sugars (D-glucose, D-mannose, D-galactose, and D-arabinose) with (3-hydrazono-2-oxo-2,3-dihydroindol-1-yl)acetic acid hydrazide 3 which was prepared from the reaction between hydrazine hydrate and (2,3-dioxo-2,3-dihydro-indol-1-yl)acetic acid ethyl ester 2. Acetylation of 4-7 afforded the per-O-acetylsugar-N-acetylhydrazones 8-11. Cu(II), Zn(II), Mn(II) and Fe(III) complexes of the glucose derivative 4 [HL] were prepared and characterized by elemental analysis, conductivity measurements, IR, UV-Vis. and magnetic moment measurements. TGA and DTA confirm the chemical formulation of the complexes and their thermal decomposition were evaluated.
(2016). Synthesis and complexation of some sugarhydrazone derived from isatin. Assiut University Journal of Multidisciplinary Scientific Research, 45(2), 58-75. doi: 10.21608/aunj.2016.221435
MLA
. "Synthesis and complexation of some sugarhydrazone derived from isatin". Assiut University Journal of Multidisciplinary Scientific Research, 45, 2, 2016, 58-75. doi: 10.21608/aunj.2016.221435
HARVARD
(2016). 'Synthesis and complexation of some sugarhydrazone derived from isatin', Assiut University Journal of Multidisciplinary Scientific Research, 45(2), pp. 58-75. doi: 10.21608/aunj.2016.221435
VANCOUVER
Synthesis and complexation of some sugarhydrazone derived from isatin. Assiut University Journal of Multidisciplinary Scientific Research, 2016; 45(2): 58-75. doi: 10.21608/aunj.2016.221435
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